HS-SPME/GC-MS-O法检测卷烟包装纸中的挥发性成分及异味成分

doi:10.14088/j.cnki.issn0439-8114.2022.22.027

湖北农业科学 ›› 2022, Vol. 61 ›› Issue (22): 152-157.doi: 10.14088/j.cnki.issn0439-8114.2022.22.027

HS-SPME/GC-MS-O法检测卷烟包装纸中的挥发性成分及异味成分

曾强¹, 朱红艳¹, 何攀¹, 王文凤², 许文璨², 孙鹏¹, 肖超¹, 祝秋¹, 王丹¹, 黄友谊², 方欣²

1.武汉虹之彩包装印刷有限公司,武汉 430040;
2.华中农业大学园艺林学学院,武汉 430077

收稿日期:2022-06-06 出版日期:2022-11-25 发布日期:2023-01-11
通讯作者: 方欣,在读博士研究生,研究方向为植物产品加工与生物技术,（电子信箱）1846380277@qq.com。
作者简介:曾强（1980-）,男,湖北武汉人,工程师,主要从事印刷材料分析及印刷适性研究工作,（电话）13343400575（电子信箱）308172017@qq.com
基金资助:
武汉虹之彩包装印刷有限公司应用技术类项目（2019JSZL3JS2C039）

Volatile components and peculiar smell components in cigarette packaging paper detected by HS-SPME/GC-MS-O method

ZENG Qiang¹, ZHU Hong-yan¹, HE Pan¹, WANG Wen-feng², XU Wen-can², SUN Peng¹, XIAO Chao¹, ZHU Qiu¹, WANG Dan¹, HUANG You-yi², FANG Xin²

1. Wuhan Hongzhicai Packaging Printing Co., Ltd.,Wuhan 430040, China;
2. College of Horticulture and Forestry Sciences, Huazhong Agricultural University, Wuhan 430077, China

Received:2022-06-06 Online:2022-11-25 Published:2023-01-11

摘要/Abstract

摘要： 为探究烟包装纸中挥发性成分和主要的异味成分,采用HS-SPME/GC-MS-O技术检测了烟包装纸印制中原纸、半成品和成品的挥发性成分以及成品中的异味成分。结果表明,从5个不同印制阶段的烟包装样品中共鉴定出106种挥发性成分,主要为芳香烃类、酯类、烃类化合物;从烟包装纸中共嗅闻鉴定出壬醛、二乙二醇丁醚、对苯二甲醚、3-甲氧基苯酚和2,5-二叔丁基-1,4-苯醌5种异味成分,异味成分主要来源于原纸、丝印裂变、凹印3个印制阶段。

关键词: 顶空固相微萃取（HS-SPME）, 气相色谱-质谱-嗅闻联用（GC-MS-O）, 卷烟包装纸, 异味成分

Abstract: In order to know the volatile and odor components in cigarette packaging paper, the HS-SPME/GC-MS-O technology was used to detect the volatile components of raw paper, semi-finished products and finished products during different printing stages of cigarette packaging paper, as well as the odor components in the finished product. The results showed that a total of 106 volatile components were identified from the samples during five printing stages of cigarette packaging paper, and their main components were aromatic family, esters, and hydrocarbons. Five odor substances, such as nonanal, diethylene glycol butyl ether, p-dimethyl ether, 3-methoxyphenol and 2,5-ditert-butyl-1,4-benzoquinone, were identified from cigarette packaging paper, which were mainly derived from three printing stages of base paper, screen splitting, and gravure printing processes.

Key words: headspace solid phase microextraction （HS-SPME）, gas chromatography-mass spectrometry-olfactory （GC-MS-O）, cigarette packaging paper, odor components

中图分类号:

S572

曾强, 朱红艳, 何攀, 王文凤, 许文璨, 孙鹏, 肖超, 祝秋, 王丹, 黄友谊, 方欣. HS-SPME/GC-MS-O法检测卷烟包装纸中的挥发性成分及异味成分[J]. 湖北农业科学, 2022, 61(22): 152-157.

ZENG Qiang, ZHU Hong-yan, HE Pan, WANG Wen-feng, XU Wen-can, SUN Peng, XIAO Chao, ZHU Qiu, WANG Dan, HUANG You-yi, FANG Xin. Volatile components and peculiar smell components in cigarette packaging paper detected by HS-SPME/GC-MS-O method[J]. HUBEI AGRICULTURAL SCIENCES, 2022, 61(22): 152-157.

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HS-SPME/GC-MS-O法检测卷烟包装纸中的挥发性成分及异味成分

Volatile components and peculiar smell components in cigarette packaging paper detected by HS-SPME/GC-MS-O method

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