湖北农业科学 ›› 2021, Vol. 60 ›› Issue (3): 125-128.doi: 10.14088/j.cnki.issn0439-8114.2021.03.024

• 检测分析 • 上一篇    下一篇

ICP光谱法分析蒲公英茶浸出物中微量元素及其溶出特性

刘冰冰, 刘佳, 张辰凌, 韩梅, 贾娜   

  1. 中国地质科学院水文地质环境地质研究所/自然资源部地下水科学与工程重点实验室,河北 正定 050803
  • 收稿日期:2020-05-26 发布日期:2021-02-25
  • 通讯作者: 贾 娜(1981-),高级工程师,主要从事水质分析研究,(电子信箱)jiana1209@126.com。
  • 作者简介:刘冰冰(1987-),女,吉林四平人,工程师,硕士,主要从事水质分析研究,(电话)15930168670(电子信箱)408729357@qq.com
  • 基金资助:
    中国地质科学院水文地质环境地质研究所基本科研业务项目(SK202004)

Analysis of trace elements in dandelion tea extract and the dissolution characteristics by ICP spectroscopy

LIU Bing-bing, LIU Jia, ZHANG Chen-ling, HAN Mei, JIA Na   

  1. Institute of Hydrogeology and Environmental Gelogy, Chinese Academy of Geological Science/Key Laboratory of Groundwater Science and Engineering, Ministry of Natural Resources,Zhengding 050803,Hebei,China
  • Received:2020-05-26 Published:2021-02-25

摘要: 建立了电感耦合等离子体发射光谱法测定蒲公英茶浸出物中微量元素Zn、Cu、Mn、Li、Ni、Pb、Sr、Cd、Fe、Ba含量的方法并研究其溶出特性。在ICP光谱仪最佳工作条件下,确定待测元素波长,测定蒲公英茶样品浸出物中微量元素并加标回收,其回收率在95.7%~104.8%,相对标准偏差(RSD)在1.0%~3.2%。冲泡和煎煮2种方法对元素的溶出量影响不大,浸出物中Sr的含量较高,其次是Mn和Zn,Cd和Pb均未检出。蒲公英茶浸出物中微量元素的溶出量随着冲泡时间的增加呈线性增加。随着冲泡次数的增加,蒲公英茶浸出物中微量元素的溶出量逐渐降低。经过2次冲泡后,除了Fe的溶出率为64.5%,其他微量元素的溶出率都在93.3%~100.0%。

关键词: ICP光谱法, 蒲公英茶, 微量元素, 溶出特性

Abstract: A method for the determination of trace elements zinc, copper, manganese, lithium, nickel, lead, strontium, cadmium, iron and barium in dandelion tea extract by inductively coupled plasma-optical emission spectrometry was established and the dissolution characteristics was studied. Under the optimal working conditions of ICP spectrometer, the wavelengths of the elements were chosen and the trace elements in the dandelion tea sample extract were analyzed with the recoveries of 95.7%~104.8% and relative standard deviation (RSD) of 1.0%~3.2%。The two methods of brewing and boiling had little effect on the dissolved amount of trace elements. The content of Sr in the dandelion tea extract was higher, followed by Mn and Zn, and neither Cd nor Pb was detected. The dissolved amount of trace elements in the dandelion tea extract increased linearly with the increase of brewing time. With the increase of the times of brewing, the dissolved amount of trace elements in the dandelion extract gradually decreased. After two times of brewing, the dissolution rate of Fe was 64.5%, and the dissolution rate of other trace elements was between 93.3%~100.0%.

Key words: ICP emission spectrometry, dandelion tea, trace elements, dissolution characteristics

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